GC/MS analysis results for sample AD23326, Oct 16 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23326.D Vial: 13 Acq On : 10 Oct 2001 1:04 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101,M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.45 ug/1 41168 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 ntative ID MW MolForm CAS# Qual 1 3-Hexanone/ 100 C6H12O 000589-38-8 91 2 3-Pentancme, 2-methyl- 100 C6H12O 000565-69-5 53 3 2,4-Pent^nedione 100 C5H8O2 000123-54-6 43 4 Butane,/2,2-dimethyl-______________ 86 C6H14 000075-83-2 42 Abundance Scan 146 (6.385 min): 23326.D (-) m/z 4^/00 100.00% 40 5,7

71 5000 100

6.00 6.20 6.40 6.60 6.80 ...... +-T +Tn-i rj-r,-, ,| t I”"IH.•I.I•II m/z 5^/95 94.22% n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone 43 57

71 5000 6.00 6,20 6.40 6.60 6.80 100 m/z 71.00 62.49%

Tl/Z-> I''''1’'''I J I.............. I' ttp-rrTr."! I'’"I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 , 85

Abundance #63398; 3-Pentanone, 2-methyl- 5(7 43 6.00 6,20 6.40 6.60 6.80 5000 m/z 100.05 377437 100 71 ft 85 I' ‘' I'''' r''' I ' I'''' I' ‘' i Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63324:2,4-Pentanedione .... .......... 43 6.00 6.20 6.40 6,60 6.80 Ppz 41705 24.21% 5000 85 100

27 38 , 58 72 ............ 11" " I" " I" 111 ■. ■ ■ I ■ ■ ■ ■ 1111111 ■ 11111 ""I.......... ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80

23326.D NP091101.M Thu Oct 11 12:58:35 2001 Page 1

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