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GC/MS analysis report, sample AD23654, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23654 showing detection of unknown compounds on October 16, 2001.

NYC-WTC_000089087–000089101

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089095
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23654.D Vial: 7 Acq On : 15 Oct 2001 6:03 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr’; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.45 ug/1 44111 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanone 100 C6H12O 000589-38-8 64 2 3-Pent^one, 2-methyl- 100 C6H12O 000565-69-5 42 3 2,4-^ntanedione 100 C5H8O2 000123-54-6 38 4 Butane, 2,2-dimethyl-__________ _ 86 C6H14 000075-83-2 28 Abundance Scan 146 (6.384 min): 23654. D (-) m/z 43.00 100.00% 413 57

71 553 100

6.00 6.20 6.40 6.60 6.80

TTfe-> ■T + P^^J ,...................85I' P^^H 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 P m/z YTTPy 56795 88771% Abundance #63358:3-Hexanone 43 57

71 5000- 6.00 6.20 6.40 6.60 6.80 100 “mTz 71.00 65721% J pM I'' " I' Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63398: 3-Pentanone, 2-methyl-

43 6.00 6.20 6.40 6,60 6.80 5000- m/z 100.05 39.02% 100 71 --------- 85- - -- I' " ' I ‘ ’ I +P^ +tpt^ P""^ Ti/z-> ~ Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85' '90' '95 100 105

43 #63324:2,4-Pentanedione-------- ---------- I —6.00-^6.20-t-6.-40—6:60—6:80~ ...... m/z-- 41T05-- 23T68% 5000- .85 100—-

27 pW 58 Itt+t- 7 I ‘' I' I'' I'''' I p Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80

23654.D NP091101.M Tue Oct 16 15:04:57 2001 Page 1

NYC-WTC_000089095

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NYC-WTC_000089095Source: NYC Law Department, mirrored locally

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