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GC/MS analysis report, sample AD23654, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23654 showing detection of unknown compounds on October 16, 2001.

NYC-WTC_000089087–000089101

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089096
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23654.D Vial: 7 Acq On : 15 Oct 2001 6:03 pm Operator; 209 GALOS Sample :' gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.99 ug/1 96933 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 'entative ID MW MolForm CAS# Qua! 1 2-Hexanonj 100 C6H12O 000591-78-6 91 2 Oxirane,/2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 64 3 Methyl sobutyl Ketone 100 C6H12O 000108-10-1 53 4 2-Hex^ one, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 42. Sundance Scan 157 (6.485 min): 23654. D (-) Tm/z 42.95 100.00% 40 58 5000

6.20 6.40 6.60 6.80 I'''' I'''' I •' ,.SX-T 7,1I b " I • ■ " I " "1" " I" " I' "T • I >" ■ I 'I m/z 58.05 58.20% Tl/Z-> 20 25 30 35 40 45 50 55 60 65 70 , 75 80 85 90 95 100 105 Abundance #1556:2-Hexanone 43

58 5000 6.20 6.40 6.60 6.80 m/z 57.00 15.35% .... T.. 27 71 ..... ,,l............. I,., tVz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1530: Oxirane, 2-methyl-2-(1 -methylethyl)- ----- ;------ —------———----------- ,--- - --- -- ----- —. 58 6.20 6.40 6.60 6.80 SsS “m/z 41.05 13.69% 71

__ ___ 30. ------- 52. -66 — ______ 85________ 100 pTTTTTTTrlrTTTpTTTpTTTp^^ I..........I' TTTTTTT+ n/2-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance ------------------- - #63354: Methyl Isobutyl Ketone ^.^.--.^1^,-^ ---------------------------- J,- -^6.20~~ 6.40~ 6.60' ~6.80------ ■fn/z 99795 11.48%

253 — 58-

85 100 67 pTT-rpT-rrjTTTTpTTTp-TTTjTTTT^^ _ p,/, ,,, I, I Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

23654.D NP091101.M Tue Oct 16 15:05:00 2001 Page 2

NYC-WTC_000089096

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NYC-WTC_000089096Source: NYC Law Department, mirrored locally

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