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GC/MS analysis report, sample AD23654, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23654 showing detection of unknown compounds on October 16, 2001.

NYC-WTC_000089087–000089101

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089097
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23654.D Vial: 7 Acq On : 15 Oct 2001 6:03 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.62 0.41 ug/1 40155 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 S-HexanoZ 102 C6H14O 000623-37-0 83' 2 3-Pent^ol ,88 C5H12O 000584-02-1 38 . 3 1,2-BXtanediol 90 C4H10O2 000584-03-2 36 4 4-Heptanol 116 C7H16O 000589-55-9 22 Abundance Scan 172 (6.622 min); 23654.D (-) m/z 59700 100.00% . 5(9 55

73 5000 4143 I , , , . I , 4,4 ' ' ' pr? . . I . . 6.20 6.40 6.60 6.80 7.00 39 '' I' ' ' ' I '' '' I '' ' ' I '' ' H I ' ' ' ' I ' ' ' ' I ' ' ' I ' ' ' ' I ' mTz 55.00 797^7%’ TTfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #63531 ;3-Hexanol

55

5000 73 6.20 6,40 6.60 6.80 7.00 43 "m/z 73.00 50.47% 39 45 57 I 1 I I • I I > I I ■ I I I I I I I I I 11' t i 11, ........... l-p-n-r-p-r Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #62943; 3-Pentanol 5b ............ (4^.......... 31 6.20 6.40 6.60 6.80 7.00 5000 m/z 43.05 26.29% 2729 41 ____ 4345____ 5557 T-r-r4-r-^d-r-rr-r-p-TT^^ 11' ■' ■ I' ■ ■ ■ I■ 1111 >. I.. TlZz-> 20 ■ 25 30 35 40 45 50 55 60 65 70 75 80 Abundance - — #62989; 1-,2-Butanediol “31-- - —?5b- - “6:20“6.40“6;60’^6:80“7.00 " m/z 41.05 24.46%

— -43 —------- 61 27 45 C7

20 25 30 33 ' ' ' I ' 35 .. I.Tv,... 40 45 50 55 1 I ' ' ' I ' ' ' ‘ I ' ' ' ' I ' ' ' ' I ' ' 60 65 70 75 80 6.20 6.40 6.60 6.80 7.00

23654.D NP091101.M Tue Oct 16 15:05:02 2001 Page 3;

NYC-WTC_000089097

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NYC-WTC_000089097Source: NYC Law Department, mirrored locally

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