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GC/MS analysis report, sample AD23717, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23717 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089171–000089184

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089181
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23717.D Vial: 13 Acq On : 15 Oct 2001 11:56 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101 .M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

6.73 0.47 ug/1 43256 1,4-Dichlorobenzene-d4 11.76

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexan( 102 C6H14O 000626-93-7 83 2 2-Pent ol, 4-methyl­ 102 C6H14O 000108-11-2 74 3 2-Hex. ol, (S)- 102 C6H14O 052019-78-0 64 4 Butai; , 2-ethoxy­ 102 C6H14O. 002679-87-0 56 A.bundance Scan 184 (6.734 min): 23717.D (-) m/z 44795 100.00% 4)5

5000-

41 69 —'' I' r ........ 84 87 6.40 6.60 6.80 7.00 TTTtt+ m/z 69.00 16.46% nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584:2-Hexanol 4^ A A / ^^A

5000 ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I 6.40 6.60 6.80 7.00 69 m/^ 41.05 15.75%

Ti/z-> Abundance 10 i,,,..... 19...... 15 20 25 30 56 . .................. a 35 40 45 50 55 60 65 70 75 80 85 90 95 #63546:2-Pentanol, 4-methyl-___________ . 8487 TTTHTr+rrp

415

■ 6.40 6.60 6.80 7.00 5000- m/z 42.95 11.91%

27 69 19 1-31 42.. I FlT/.TT./! m ~..... •n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance - #1769: 2-Hexanol, (S)- J— —415—----------------- 6.40 .6.60—6.80: .7.00__ 1 m/z 43.95 10.07%

5000

55 8487 TTpTTT-pTTTyTTTTprrTtpTT-rpTT-rp-rr^^ n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 ’ 85 90 95 6.40 6.60 6.80 7.00

23717.D NP091101.M Tue Oct 16 15:12:06 2001 Page 3

NYC-WTC_OOo689181

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NYC-WTC_000089181Source: NYC Law Department, mirrored locally

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