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GCMS analysis results, sample AD24048, October 29, 2001

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of environmental sample AD24048 conducted on October 29, 2001, identifying unknown compounds.

NYC-WTC_000067840–000067854

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C;\HPCHEM\1\DATA\OCT2501\24048.D Vial: 9 Acq On : 25 Oct 2001 8:30 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.59 0.43 ug/1 72307 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexai^l 102 C6H14O 000623-37-0 78 2 3-Pen^nol 88 C5H12O 000584-02-1 42 3 3-Hy^oxy-3-methyl-2-butanone 102 C5H10O2 000115-22-0 38 4 3-Pentanol, 2-methyl- 102 C6H14O 000565-67-3 38 Abundance Scan 169 (6.592 min): 24048.D (-) m/z 59.05 100.00% 50

5000 73 43 --n ■’

84 100 6.20 6.40 6,60 6.80 7,00 4

JL I ' ' ' '‘I I'' ' ■ I ■ I ■ ■ I • ■ ■ • I • ■ ■ ■ I ra/z 55.00 85.96% TiZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63527:3-Hexanol 50

5000 73 31 6.20 6.40 6.60 I6.80 7.00 m/z 73.00 44.98% I 4I'r ■.■ri 84 ' I ' ' ' ' I TiZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62942; 3-Pentanol 50 ............................... { I (^11111111

31 6.^ 6.40 6.^ 6.^ 7.00 5000 m/z 43.00 31.02% 41

_______ 87_______________ -

-,,.. Az ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ‘ ' I Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63477:3-Hydroxy-3-methyl-2-butanone 50 =n^ 6.20 6.40 6.60 6.80 7.00 m/z41.0522.69% 5000 31 43 15 rT-T-A—ryn—r-Ar-^^T—i-r-r-p4-0- 'T' ■ '''‘I - ' I ' ' ' ' I ‘ v' 1 ' ' ' ' 102 I ‘ ,_ ' I Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 6.20 6,40 6.60 6.80 7.00

24048.D NP101901.M Fri Oct 26 10:20:51 2001 Page 3

NYC-WTC_000d67850

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NYC-WTC_000067850Source: NYC Law Department, mirrored locally

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