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GCMS analysis results for sample AD24047, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24047 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067826–000067839

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24047.D Vial: 8 Acq On : 25 Oct 2001 7:31 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.69 0.42 ug/1 66431 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-Hexanol 102 C6H14O 000626-93-7 83 2 2-Pentan , 4-methyl- 102 C6H14O 000108-11-2 64 3 2-Butam 74 C4H10O 000078-92-2 39 4 2-Hept ■Ol, (S)-_________________________ 116 C7H16O 006033-23-4 39 Abundance Scan 180 (6.694 min): 24047.D (-) m7z 44.95 100.00% 43

5000

69 41 8487 6.40 6.60 6.80 7.00 TTrftSy 1" 111' I" I m/z 69.00 18.42% tTiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584:2-Hexanol 4b

5000 . I . 1 .1 6.40 6.60 6.80 7.00 69 m/z ■43.05 11.79% I " '' I " " I " ‘' 1 ‘' I " •' I' ' ‘' tnfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance

AJ #63546:2-Pentanol, 4-methyl- 4)5

6.40 6.60 6.80 7.00 5000 “m/z 41.00 11777%

27 19 ) 31 42 57 8487 Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 \bundance #334:2-Butanol 4)5 _6^ 6.60 6.80 zoo m/z 43.95 6.96% 5000

27 31 59 19 55 73 I" " 1' “ ■ I" " I" “ I" I ‘' I" ■ 11'" • I ’ I" 11"' I"' ‘ I ‘ I 11 ■ • 1'" ’ I''' 11"'' I “ • ‘ 1"'' Tl&-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

24047.D NP101901.M Fri Oct 26 10:17:31 2001 Page 3 NYC-WTC_000067836

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NYC-WTC_000067836Source: NYC Law Department, mirrored locally

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