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GCMS analysis results, sample AD23915, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23915 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067635–000067650

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File j C:\HPCHEM\1\DATA\OCT1701\23914.D Vial: 12 Acq On : 18 Oct 2001 12:03 am Operator: 209 GALOS Sample : gc/ms unknown Inst s GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.40 ug/1 40982 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 tentative ID MW MolForm CAS# Qual 1 3-Hexanol 102 C6H14O 000623-37-0 74 2 3-Pentan 88 C5H12O 000584-02-1 36 3 3-Pent 1, 2-methyl- 102 C6H140 000565-67-3 36 4 1-Hept: -4-ol 112 C7H12O 022127-83-9 10 Abundance ? Scan 172 (6.623 tnin): 23914.D (-) m/z 59705 100.00% 5b

5000 73 43 .6.{5 ' n ■ ' ' ' I ' 6.20 6.40 6.60 6.80 7.00 84 Wz 55.00 87.99% ■nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #63529:3-Hexanol 5b

5000 31 73 6.a3 6.40 6.60 6.80 7.00 “mTz 73.00 46.41% 44 T T-+ I" " I'I +u n*"’ T 102 Ttfe-> 20253035404550556065 70 7580859095 100105 110 Abundance #62943:3-Pentanol sb 6.^ 6.M 6,80 '7.66 31 500) m/z 42.95 37.33% 41

p-rT.|lll.|..,,|,rTThll T r Tlfe-> 20 25 30 35 40 45 50 55 a) 65 70 75 80 85 90 95 100 105110 Abundance #63561:3-Pentanol. 2-methyl- I , , . . I . I . I I I , > I I . .n I I . i ' 5b 6.20 6.40 6.60 6.80 7.00 “m/z 41.05 24.30%

JuUu. 5000 73 31 45 4 85 ’ I' ’" I' ‘* I ‘' 1 ‘ 102 ’ 1 *" ’ 1'' “T' * ’' 1 ’ ' 6.ro'' ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.^ " '7.00

23914.D NP101901.M Wed Oct 24 11:14:58 2001 Page 3 NYC-WTC_000067645

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NYC-WTC_000067645Source: NYC Law Department, mirrored locally

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