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GCMS analysis results, sample AD23915, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23915 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067635–000067650

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1701\23914.D Vial: 12 Acq On : 18 Oct 2001 12:03 am Operator: 209 GALOS San^le : gc/ms unknown Inst ! GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method s C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.87 ug/ 88355 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 tntative ID MW MolForm CAS# Qual 1 2-Hexanon^ 100 C6H12O 000591-78-6 91 2 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 QxiranX, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 50 Abundance / Scan 158 (6.495 min): 23914.D (-) Wz 43.00 100.00% 43

58 5000

1 ’ * * ' I ’ ' ' ' 1 * ’ * ’ I 85 100 6.20 6.40 6.60 6.80 1, , IT, , I ,l|l| 51 k 71 I 1 I ' ' ' ' I ' ' ‘' I ' ' ‘' I ' m/z 58.05 56.15% TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63387:2-Hexanone 43

5000 58

100 m/z 6J20 i. 6,40 6.60 6.80

71 85 I ' ' ' ■ I ' M ,-1 |l J. ’ I ’ ' ‘ ' I ' . ........... I..|. tiZz-> 20 30 40 50 60 70 80 90 100110lSl30140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.20 6,40 6.60 6.80 5000 29 "m/z 41.00 12.00%

' I'''' I'' >' 11 ,1,60 ’ 1 ‘ 50 ’ 1 ' 71 85 100 140 iiZz-> 20 30 40 70 80 90 100 110 120 130 140 Abundance Methyl Isobutyl Ketone 43 6.2) 6.40 6.ot' 'rto' ' m/zl00.05i 11.32% 5000 58 I 27 I I, ' I ' * ‘ * 1 ‘ 67 ' ' I '' '' I ‘ 85 I ‘ ‘ I' 100

n/z-> 2030 40 50 60 70 80 90 1001101M130140 6.20 6.40 6.60 6.80

23914.D NP101901.M Wed Oct 24 11:14:56 2001 Page 2 NYC-WTC_000067644

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NYC-WTC_000067644Source: NYC Law Department, mirrored locally

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