GC/MS analysis report for sample AD25839, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1901\25830.D Vial: 4 Acq On : 19 Nov 2001 6:12 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.43 ug/1 92521 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm , CAS# Qual 1 2-Hexanone / 100 C6H12O 000591-78-6 91 2 2-Hexanoney^-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 Methyl Isdbutyl Ketone 100 C6H12O 000108-10-1 59 4 2-Hexang<ne, 5-methyl- 114 C7H14O 000110-12-3 39 ^bundance Scan 151 (6.434 min): 25830.D (-) m/z 42.95 100.00%! 43

58 5000

100 71 85 6.00 6.20 6.40 6.60 6.80 I I "mTz 58.0.5 57774% Ti^-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63387:2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 100 m/z 100.05 18.68% 71 II ' I' ‘' I ' ’ ’' I ' 20 30 40 50 60 70 80 90 100 110 120 1M140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyV 43 \An “-fT-TT-T-p-r 58 6.00 6.20 6.^ 6,^ 6.80 5000 29 m/z 41.05 18.23%

100 'I' ''‘I I ,1, ' I ' ' ' ■ I ' 71 85 140 Tife-> 20 30 40 50 60 70 80 90 100 1101M130140 Abundance #63349: Methyl Isobutyl Ketone 43 6.00 6.20' ' 6.^' ' 6.60' ' 6.80' m/ z 57.00 14.06% 5000 58

85 100 67 I T,Zz-> 20 30 40 50 60 70 80 90 100^1^120130140 6.66' 6.40 6.^' 6.ro

25830.D NP103001.M Wed Dec 05 15:27:23 2001 Page 1

NYC-WTC_000070132