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GCMS analysis results for sample AD24641, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24641 with detection of unknown compounds on November 13, 2001.

NYC-WTC_000068672–000068683

Folder label: “508 Scan X 10/16/01 A 11/5/01

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Scanned page image, NYC-WTC_000068680
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24641.D Vial: 11 Acq On : 5 Nov 2001 9:44 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.54 ug/1 100535 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone/^ 100 C6H12O 000591-78-6 90 2 2-Hexanope, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 Methyl/fsobutyl Ketone 100 C6H12O 000108-10-1 52 4 Prop .al 58 C3H6O 000123-38-6 43 ^bundanceX Scan 151 (6.428 min): 24641 .D (-) m7z 42.95 100.00% 43

58 5000

71 85 iw 6,00 6.20 6.40 6.60 6.80 m/z 58.05 52.39% 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556:2-Hexanone 43

58 5000 I ' ' ' ' I ' 'I ' I ' ■ I 6,00 6.20 6.40 6.60 6.80 “m/z 41.05 16.17% 27 71 85 100 ........ ‘ I' ' ' I ' TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43

58 6;OoaM_a4g__6;6o__6jo_ 5000 29 "m/z 57.00 14.36%

' P ' ' ' I ' ' ' ' I I J 71 I 85 4^ 100 140 T}/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63351: Methyl Isobutyl Ketone 4)3 6,00 6.20 6.40 6.60 6.80 m/z 100.05 11.59%

5000 58

JU 20 30 40 ,

50 T

60 , 72, , 70 80 85 100 I......... I......... . , , I............... 90 100 110 120 130 140 \ AA

6.00 6.20 6.40 6.60 6.80

24641.D NP103001.M Fri Nov 09 12:16:12 2001 Page 1

NYC-WTC_000068680

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NYC-WTC_000068680Source: NYC Law Department, mirrored locally

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