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GCMS analysis results for sample AD24052, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24052 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067894–000067907

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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Scanned page image, NYC-WTC_000067903
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24052.D Vial: 13 Acq On : 26 Oct 2001 12:25 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C;\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.46 0.89 ug/1 170551 1,4-Dichlorobenzene-d4 11.74 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 91 2 2-Hexaj^one, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 MethyX Isobutyl Ketone 100 C6H12O 000108-10-1 52 4 2-Hexanone, 5-methyl- 114 C7H14O 000110-12-3 38 <\bundanc8 Scan 154 (6.461 min): 24052.D (-) m/z 42.95 100.00% 43

58 5000

.,,51 I, 71 85 1^ 6.20 AJ 6.40 6.60 6.80 ' ' ' I l. I 111 11.. I ■ . I.... I. I.. I. ... I . 11 ■ I... i I. I m/z 58.05 54.82% TiZz-> 20 30 40 TO TO 70 TO 90 100 110 120 130 140 (Abundance #63387:2-Hexanone 43

58 5000 6.20I 6.40 6.60 6,80 100 m/z )57.00 15.08% 85 I 71 I I

I'V r" " I " + Tife-> 20 30 40 50 ' 70 ‘ to " "ioo“il6"i^"w' 'l40 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.20 6.40 6.60 6.80 5000 29 m/z 41.00 13.76%

100 ' I '' ■' I' ■ ■ ' 11 J. 71 I 85 ( I* ' • ' 1 ’ ’ ' 4^ 140 Tife-> 20 30 40 50 60 70 80 90 100 "i^ Mxindance I; Methyl Isobutyl Ketone 43 6.20 6.40 6.60 6,80 m/z 100.00 11.28% 5000 58

I 67 TO ' TO "^O 85 I,, 100

Tife-> 20 30 40 TO 90 100 110 120 130 140 '6.TO RTO 'e.TO 6.TO

24052.D NP101901.M Fri Oct 26 10:32:14 2001 Page 2

NYC-WTC_000067903

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NYC-WTC_000067903Source: NYC Law Department, mirrored locally

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