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GCMS analysis results for sample AD24049, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24049 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067855–000067866

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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Scanned page image, NYC-WTC_000067863
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24049.D Vial: 10 Acq On : 25 Oct 2001 9:29 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.47 0.65 ug/1 130685 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 90 2 2-Hexanone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 74 3 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 ^bundance Scan 156 (6.473 min): 24049.D (-) m/z 42.95 100.00% 4)3

58 500)

71 85 IM 6.20 AJ 6.40 6.60 6.80 +t -rkTTpT-rTpTTT-)TT-rTpTTTJTTTTjTTTTpT^^ ra/z 58.05 55.63% TTfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1556:2-Hexanone 43

58 I 1 r*! 1 I i7^p-rTT I* r I । i 5000 6.40 6.60 6.80 m/z 41.00 17.59% 27 71 85 100

Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 M. .. Abundance #15807:2-Hexanone, 4-hydroxy-5-m8thyl-3-propyk

6.20 6.40 6.60 6.80 5000 “mTz 57700 15.84% 58 27 72 I 85 100 TTyt+r .. . I" " 1 Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 (Abundance #63350: Methyl Isobutyl Ketone 4|3 6.20 6.40 6.60 6.80 m/z 100.05 10.42% 5000 58

85 iw 67 ‘ ' I ' ' ' ' I ' ' *'1'■ ■ ■ I ' I ‘ I ‘I" 20 25 30 35 40 45 50 55 60 65 70 75 80 85 30 95 100 105 6.20 6.40 6.60 6.80

24049.D NP101901.M Fri Oct 26 10:23:22 2001 Page 1 NYC-WTC_000067863 ’

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NYC-WTC_000067863Source: NYC Law Department, mirrored locally

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