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GC/MS analysis results for sample AD23324, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.

NYC-WTC_000088316–000088345

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088324
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1201\23324.D Vial: 17 Acq On : 12 Oct 2001 5:46 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.96 ug/1 95898 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 . Tentative ID MW MolForm CAS# Qual

1 2-Hexanonfe 100 C6H12O 000591-78-6 91 2 2-Hexanqne, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 72 3 MethyyIsobutyl Ketone 100 C6H12O 000108-10-1 58 4 Oxiryie, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 50 Abundance / Scan 158 (6.489 min): 23324. D (-) Wz 42795 100.00% 43

58 5000 AJ nZz-> I,. ..... 41 20 30 40 50 60 71

70 80 85

90 100 ........................................ 100 110 120 130 140 m/z 6.20 6.40 58.05 6.60 6.80 56.75% Abundance #1556:2-Hexanone 43

58 ... I ,,, q ,,,, I ,,,,,,,, , 5000 6.20 6.40 6.60 6.80 “mTz 41.05 16.83% 27 71 85 100 I. I . . ,1, , . . . ,i| |l Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43

58 _6^ 6.40 6.60 6.80 Sigi] 29 m/z 57.00 15.60%

' I ' ‘ ' ' I ' ' ' ' I I J. ' I'''' I' 71 85 100 I I'l 11111 i‘i 11111 > 11111111111111111 140 Tl/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63354: Methyl Isobutyl Ketone 43 6.20 6.40 6.60 6.80 m/z 100.05 9.38% 5000 58 85 100

Tl/Z-> .. i 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.80

23324.D NP091101.M Mon Oct 15 10:33:23 2001 Page 2

NYC-WTC_000088324

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NYC-WTC_000088324Source: NYC Law Department, mirrored locally

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