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GC/MS analysis report, sample AD23723, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23723 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089259–000089272

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089268
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23723.D Vial: 19 Acq On : 16 Oct '2001 5:46 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.86 ug/1 83901 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 -Tentative ID MW MolFonn CAS# Qual 1 2-HexanoKfe i 100 C6H12O 000591-78-6 91 2 2-Hexa: me, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Methy^ Isobutyl Ketone 100 C6H12O 000108-10-1 ’58 4 Oxir^e, 2-methyl-2- (1-methylethyl) IQQ C6H12O _____ 072221-^325 50 Abundance Scan 158 (6.494 min): 23723.D (-) m/z 42.95 100.00% 43

58 5000

71 85 100 6.20 6.40 6.^ 6.80 50 .1, I m/z 58.05 60.68% Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556:2-Hexanone 43

58 5000 ' . ' I .... 6.20 6.40 6.60 6.80 m/z 41.00 18.21% 27 ........ I ■nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.20 6.40 6.60 6.80 5000 29 m/z 57.00 16.08%

100 ---------- J. 71 Ui 85

120' '130 '140 TiZz-> 20 30 40 50 60 70 80 90 ioo' i-io' - ——A Abundance #63351: Methyl Isobutyl Ketone 43 - — ^6.20-^-6.40 — 6.60 — 6.80—— ^-m/z--^100v05-^ ■“12t64%

553 58 _

■n/2-> JU 20 30 40 I'' 50 i‘i' 60 72 70 80 85 I 90 100 [ 100 110 120 130 140 6.20 6.40 6.60 6.80

23723.D NP091101.M Tue Oct 16 15:18:51 2001 Page 2

NYC-WTC_000089268

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NYC-WTC_000089268Source: NYC Law Department, mirrored locally

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