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GC/MS analysis results for sample AD23324, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.

NYC-WTC_000088316–000088345

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088325
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1201\23324.D Vial: 17 Acq On : 12 Oct 2001 5:46 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexahol Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T. 6.63 0.47 ug/1 46796 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm' CAS# Qual

1 3-Hexanol / 102 C6H14O 000623-37-0 83 2 3-Pentanol 88 C5H12O 000584-02-1 53 3 1,2-ButXnediol ( 90 C4H10O2 000584-03-2 36 4 4-HepJzanol 116 C7H16O 000589-55-9 10 Abundance Scan 173 (6.627 min); 23324.D (-) ■m/z 59705 100.00% 55

5000 73 43 39 6.20 6.40 6.60 6.80 7.00 I , , 49 I'''' I'''' I'''' I +t +4- I. ^.1 ’ I'' " I'''' J ''' I ‘' I "m/z 51775 81.08% tVz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ^bundance #63531:3-Hexanol

55

5000 73 6.20 6.40 6.60 6.80 7.00 43 m/z , 73.00 47.23% 39 I'''' I'''' I T4Tr4+trrrTTT +4 I'' ‘' I nZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #851; 3-Pentanol 5)9

31 6.201 6.40 6.60 6.80 7.00 So. m/z 43.00 25.63% 27 41 15 T-+ 4^ I'''' I' " ' I'''' I''' ‘ I I''" I Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90' Abundance #62989; 1.2-Butanediol 31 5|9 6.20 6.40 6.60 6.80 7.00 m/z 41.00 21.07%

5000

43 27 " I" " 1" " I" " I’ I" I . |47 t-r|niiHilll|7iirp-rii|i-ll 55,1 11"' I" " I' "' I'"' I" '' I' ‘" I " " I tVz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.20 6.40 6.60 6.80 7.00

23324.D NP091101.M Mon Oct 15 10:33:26 2001 Page 3

NYC-WTC_000088325

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NYC-WTC_000088325Source: NYC Law Department, mirrored locally

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