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GC/MS analysis results for sample AD22773, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22773 conducted on October 11, 2001, noting other unknown compounds.

NYC-WTC_000087417–000087432

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087430
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22773.D vial: 20 Acq On : 29 Sep 2001 7:04 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.48 ug/1 55370 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanoy 102 C6H14O 000626-93-7 83 2 2-Pentahol, 4-methyl- 102 C6H14O 000108-11-2 83 3 2-Butahol 74 C4H10O 000078-92-2 56 4 2-But^ol, (R)- 74 C4H10O 014898-79-4 50 Abundance7 Scan 184 (6.726 min): 22773.D (-) m/z 44.95 100.00% 4f=3

5000

69 T 41 6.40 6.60 6.80 7.00 51 m I 73 8487 ' ‘ I I' i i I • ■ " ) 111111111| 11 i l-frn 111 I I I I I 11 I■(■l 11 I I I I 111 I m/z 69.00 16.05% TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1792: 2-Hexanol 4)5

5000 6.40 6.60 6.80 7.00 Wz 41.05 11.41% 5558 f 8487 ....... .............. •••I'>"I"11I,,1,II■1II.■HII11.I,■■1I1II.I.,■,I1 TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Pentanol, 4-methyl- 4)5

6.40 6.60 6.80 7.00 5000 m/ z 9.65%

27 69 4: tVz-> 19 3^ ..... . ................ I 8487 ........ .. 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62568: 2-Butanol 4)5 6.40 eeo 6.^ 7.00 m/z 44.00 9.16% 5000

27 59

tt/z-> I'' ■' I''" I'''' H 10 15 20 25 1 30 35 40 45 50 55 60 65 70 75 80 85 90 95 72 6.40 6.60 6.80 7.00

22773.D NP091101.M Fri Oct 05 14:23:53 2001 Page 3

NYC-WTC_000087430

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NYC-WTC_000087430Source: NYC Law Department, mirrored locally

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