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GCMS analysis report, sample AD22558, October 2001

Machine-extracted title · confidence 75%

Gas chromatography-mass spectrometry analysis of sample AD22558 started October 1, 2001, identifying other unknown compounds.

NYC-WTC_000067406–000067424

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\22558.D Vial: 3 Acq On : 17 Oct 2001 3:08 pm Operator: 209 GALOS Sample : gc/ms unknown re extracted Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.67 ug/1 63786 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanol / 102 C6H14O 000626-93-7 83 2 2-Pentano]G 4-methyl- 102 C6H14O 000108-11-2 74 3 2-Hexano/, (S) - 102 C6H14O 052019-78-0 64 4 2-Butay51 74 C4H10O 000078-92-2 50 ^bundanc8 < Scan 184 (6.732 min): 22558.D (-) Wz 44.95 100.00% 4)5

5000

41 69 T 5053 ^59 I 6,40' 6.60 6.80 7.00 llll|l■ll|ll.l|ll■■|llll|llll|ll■■|■■ll|ll■q-^lll m/Y" 69.00 16.07% T)fe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584:2-Hexanol 4)5

5000 A [ " 6.^ RM 6.40 7.00 m/z 42.95 13.96%

TiZz-> Abundance 10 ....... ,:*^i ’ ’ I ’''' 1'' ’ * I ’ ’ ‘ ’ I' * * ‘ 1'' ‘ ’ 15 20 25^)35 40 45 50 55 60 65 70 75 80 85 90 95 #63546:2-Pentanol, 4-methyl- ... T......... 4)5 jy6.40 6.60 6.80 7.00 5000 m/z41.0513.39% 27 69 42 ] 8487 ■nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1769:2-Hexanol. (S)- 4b 6.40 6.60 6.80 7.00 "m/z 44.05 10.38% 5000

19 ,29 3942, 69 55 8487 ” H ‘‘ I' ‘* I' * “ I' mZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 a^io' 's-ct' '7.06

22558.D NP101901.M Tue Oct 23 15:08:20 2001 Page 4

NYC-WTC_000067417

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NYC-WTC_000067417Source: NYC Law Department, mirrored locally

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