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GCMS analysis results for sample AD23996, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD23996 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067767–000067781

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\23996.D Vial: 4 Acq On : 25 Oct 2001 3:37 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol, (R)- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.70 0.60 ug/1 114563 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanol, .7R)- 102 C6H14O 026549-24-6 83 2 2-Hexanol 102 C6H14O 000626-93-7 83 3 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 74 4 2-Hexanol, (S)- 102 C6H14O 052019-78-0 64 ^bund^e Scan 181 (6.703 min): 23996.D (-) m/z 44795 100.00% 4)5

5000

I I I '1 I I titt- 69 6.40 6.60 6.80 7.00 m/z eyroF 14.46% Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1001 (» Abundance #1794:2-Hexanol, (R)- 4)5

5000 . Cfl til 11 . 6,40 6.60 6,80 7.00 in/z 41.05 13.26% .... IV,-,|„^r.,l . 55.... 7..... 87........ T»Zz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance #63584:2-Hexanol 'Ils ‘ '7.66' 5000 m/z 42.95 12782%

56 ? 87 Tife-> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 IK #63546:2-Pentanol. 4-methyl- 4|5 AJ.... 6.40 6.60 6.80 7.00 m/z 44.00 9.33% 5000

27 69 .....19 ................. ....... 1....... 87......... nA:-> 10 15 20253035404550 55 60 65 70 75 80 85 90 95 100105 6.40 6.60 6.80 7.00

23996.D NP1019-01.M Fri Oct 26 10:09:45 2001 Page 4

NYC-WTC_000067778

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NYC-WTC_000067778Source: NYC Law Department, mirrored locally

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