GCMS analysis results for sample AD23996, Oct 29 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\23996.D Vial: 4 Acq On : 25 Oct 2001 3:37 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.72 1.93 ug/1 366330 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone,<4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 38 2 Morpholip^ 4-methyl- 101 C5H11NO 000109-02-4 9 3 Acetope^ 58 C3H60 000067-64-1 9 43-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 292 (7.722 min): 23996.D (-) m/z 42.95 100.00% 4(3

5000

Tife-> Abundance 10 20 30 3q.i ' * I ' 40 50 53 ,, ' I ■ -'''I'l 60 69 59

70 77 83 80 #64275:2-Perrtanone, 4-hydroxy-4-methyl- 90 J 100 101

110 JI7-40 m/z 7.60 55705 7-80 8.00 53.44%

413

5000 59 7.40 7.60 7.80 8.00 m/z 101.05 23789% 15 31 101 ......... I, I I 83 ‘ I ' * ‘ * i ‘ I—J—I—I—I—I—I—I—I—J—I—I—I—I—J—1 Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine. 4-methyl- 413

7,40 7.M 7.^ 8,00 5000 m/z”” 58.05 17.39% 101 71 I 56 I , , I , , |‘i , , ■ I , , , , | , |l, , , , I TiZz-> 10 20 30 40 50 60 70 80 90 100 110 Mjundance Acetone ................... , . . , , I , I ‘Ils 7.40 7.60 7.80 8.00 m/z 41.05 8.06% 50)0 58 27 I I I 1 ■ ■ • I 1 ' ' I ' ' ' ' 1 ' ' ' ‘ I ' ' ‘ ' I ‘ ' I Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 7.^' '7.^' '7.^' 8.60

23996.D NP101901.M Fri Oct 26 10:09:46 2001 Page 5

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