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GCMS analysis results for sample AD23995, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067752–000067766

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\23995.D Vial: 3 Acq On : 25 Oct 2001 2:39 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.71 1.74 ug/1 275347 l,4-Dichlorobenzene-d4 11.74 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone,-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 47 2 3-Hydroxy-2^-pentanone 102 C5H10O2 003142-66-3 9 3 5-Hexen-2'^one 98 C6H10O 000109-49-9 9 4 Morpholj/ne, 4-methyl-______________ 101 C5H11NO 000109-02-4 9 abundance Scan 291 (7.714 min): 23995.D (-) m/z 42.95 100.00% 4(3

59 5000 101 ' ' ' I ' ‘ J . ' I ‘ f‘ 1 ‘ ‘ ‘ ' 1 ‘ ‘ 1 7.40 7.60 7.80 8.00 I ‘ ‘ ‘ I * ‘ ' I ‘ 36 I ‘ I ' I. 69 m/z 59.05 51.33% ■nfe-> 10 20 30 40 50 60 70 80 90 100 110

L Abundance #64274:2-Pentanone. 4-hydroxy-4-methyl- 4^

5000 59 ' ‘zro '7.^‘ 8.00 m/z 100.95 22.67% 27 101 I I 08 Tlfe-> 'l'o‘ ‘20 ' ‘ I ' ‘ ‘ ‘ 1 ' I ' 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 519

7.60 7.80 8.00 5000 m/z 58.05 16.97% 45 15 I np 66 73 84 I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I ' 102 Tife-> 10 20 30 40 50 60 70 ao 90 ion 110 Abundance #63205:5-Hexen-2-one ' ’ I * • ’ • I ' ' ’ ’ I ‘ ‘ • I 40 7.40 7.60 7.80 8.00 m7z 41.05 7?^ 5000

55 15 27 I I 50. I_______ 83 98 I ' ' ■ ‘ I ' ' ‘ ‘ I ' ' I ‘ ' I ' ' ' ' I ' ' ' ‘ I ' ' ' ' I ‘ ' I ' ' ‘ ' I I Tlfe-> 10 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8,00

23995.D NP101901.M Fri Oct 26 10:08:22 2001 Page 5

NYC-WTC_000067764

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NYC-WTC_000067764Source: NYC Law Department, mirrored locally

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