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GCMS analysis results for sample AD23995, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067752–000067766

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\23995.D Vial: 3 Acq On : 25 Oct 2001 2:39 pm Operator: 209 GALOS Sarr^le : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanol, 4-methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.69 0.49 ug/1 78393 1,4-Dichlorobenzene-d4 11.74 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanol, -methyl- 102 C6H14O 000108-11-2 64 2 2-Hexanol y 102 C6H14O 000626-93-7 64 3 2-Hexanol< (R) - 102 C6H14O 026549-24-6 64 4 2-HexanXL, (S)- 102 C6H140 052019-78-0 64 Abundance / Scan 179 (6.686 min): 23995.D (-) m/z 44.95 100.00% 4h3

5000

69 -- rT-r-p-r-rTr-i-rT-r-rTyT^==^^ 6.40 6,60 6,80 7.00 .........56........................................ ...................... ^Illl 51 87 100 m/z 69.00 16.33% •nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63547:2-PentanoI, 4-methyl- 4|5

5000 6.40 6,60 6,80 7.00 27 -rTTTTTTrjjpTTTTTrX^rrTpTTTTTTT+T^^ m7z 41.05 13.14% ....... 38 II Tlfe-> 1'0 15 3b 35 4b 4^"»"^"ro"^'^^"^"I'ooios" Abundance #63583:2-Hexanol 4|5

6,^ 6.60 6.^ 7.00 5000 m/z 42.95 10.46%

27 39 69 55 87 TiZz-> Abundance 10 15 20 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #1794:2-Hexanol. (R)- 4t5 Ju m/z 6.40 6,60 44.00 6,80 7,00 9.04% 5000 A n&-> ” 6.TO ' 7.ro

23995.D NP101901.M Fri Oct 26 10:08:20 2001 Page 4

NYC-WTC_000067763

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NYC-WTC_000067763Source: NYC Law Department, mirrored locally

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