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GC/MS analysis results, sample AD24482, November 2001

Machine-extracted title · confidence 75%

Gas chromatography-mass spectrometry analysis of sample AD24482 completed November 13, 2001, identifying other unknown compounds with violations referenced in comments.

NYC-WTC_000068748–000068762

Folder label: “GCMS Scan X 10/15/01 A 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV0201\24482.D Vial: 21 Acq On : 3 Nov 2001 10:28 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanol, 4-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.66 0.57 ug/1 80723 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 2-Pentan^, 4-methyl- 102 C6H14O 000108-11-2 78 2 2-Hexanol 102 C6H14O 000626-93-7 64 3 2-Octanral 130 C8H18O 000123-96-6 40 4 2-Oct^ol, (R) - 130 C8H18O 005978-70-1 40 Abundance Z Scan 176 (6.662 min): 24482.D (-) m/z 44.95 100.00% 40

5000

69 87 6.40 6.60 6.80 7.00 ............. ?il,ll 56 I 98 ' ' I ' ' ' ' I ' ‘ ' I ' “mTz 41700 18.47% nfe-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63547: 2-Pentanol. 4-methyl- 45

5000 6.40I 6.60 6.80 7.00 27 m/z i69.00 15.32% 1, , ........ I, , , , ,38 ||| 57 ' I ' ' I ‘ I ' 69 ,1,.. ............ fl tVz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63584:2-Hexanol 4 , A , , 1 11 I 6.40 6.60 6.80 7.00 5000 "mTz 43795 12.12%

69 19 27 5,6 I , i-|-rT-H-T-f-rT-T-rYT-r-rT-|-H-rS-p-rT-r-p-T-r-r-|--r-r--r-r-|-r 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #65286: 2-Octanol 4□ 6.40 6.60 6.80 7.00 m/z: 42.95 10.83% 5000

nfe-> 27 .......................................... 10 20 30 40 ' I 50 57 I ' 60 70 70 80 84 90 97 ' I ' ' ' ' I ' 100 110 112 120 JJ , , 1 1

6.40 I

6.60 6.80 7.00

24482.D NP103001.M Fri Nov 09 14:54:35 2001 Page 4

NYC-WTC_000068759

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NYC-WTC_000068759Source: NYC Law Department, mirrored locally

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