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GC/MS analysis results for sample AD22917, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22917 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087586–000087598

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0201\22917.D Vial: 7 Acq On : 2 Oct 2001 7:59 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplrj 1,00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanol, 4-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.43 ug/1 49120 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 74 2 2 -Hexa^l 102 C6H14O 000626-93-7 74 3 2-He3^ol, (S)- 102 C6H14O 052019-78-0 64 4 2-H0anol, (R) -_______________ 102 C6H14O 026549-24-6 40 Abundance ' Scan 184 (6.727 min): 22917.D (-) m/z 44795 100.00% 40

5000

41 69

tVz-> 10 15 56 I" " H ' I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ,4^ 84 87 P’ 6.40 m/z 6.60 69.00 6.80 7.00 16.39% Abundance #1773; 2-Pentanol, 4-methyl- 4$

5000 6.40 T 6.60 Ck 6.80 7.00 69 m/z 41.05 11718% 27 42 I'''' I'''' I' I'' I I 8487 " 111111HI■11111111.1(II111 ■ 11111 ■ 111 ■ 11,1111111

■nlz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63582; 2-Hexanol 4(5 ‘H’

6.40 6.60 6.80 7.00 5000 m/T” 44.00 11.69%

27 19 31 57 8487 rp-m-p- p+U .. 'I".. 80' 85''90 "95 ■n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 'Abundance #1769: 2-Hexanol, (S)- ' ' I ' ' ' ' I ' ' ’ ’ I 40 6.40 6.60 6.80 7.00 m/F* 11.38%

5000

Ti/z-> 10 15 55 8487 '' U '' ‘ I'''' I''' 11'''' I'''' I'''' I'''' I'''' I ‘ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 JVJ 6.40 6.60 6.80 7.00

22917.D NP091101.M Wed Oct 03 11:07:57 2001 Page 2

NYC-WTC_000087595

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NYC-WTC_000087595Source: NYC Law Department, mirrored locally

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