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GC/MS analysis results for sample AD22917, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22917 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087586–000087598

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087594
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0201\22917.D Vial: 7 Acq On : 2 Oct 2001 7:59 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.50 ug/1 56208 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexan<^e 100 C6H12O 000591-78-6 91 2 2-Hexa^ne, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 2-Hep^none, 7,7-dichloro- 182 C7H12C12O 000000-00-0 53 4 MethyT Isobutyl Ketone___________ 100 C6H12O 000108-10-1 49 Abundance / Scan 157 (6.479 min): 22917.D (-) m/z 42.95 100.00% 43

TiZz-> 553

20 30 440 50 50 58

60 71 85 ■A-... p-,1..,-. 70 80 90 100 100

110 120 130 140 m/z 6.20 AJ 6.40 58.05 L 6.60 6.80 58.35% Abundance #1556; 2-Hexanone 43

58 . , , . I , . . Cl /, . , I 5000 6.20 6.40 6.60 6.80 “mTz 41.00 18.16% 27 7^8^ 1“ ............. l’.............. I ,

Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.20 6.40 6.60 6.80 5000 29 m/z 57.00 16.37%

TiZz-> A.bundance 20 ' I ' ' ' ' I • ' ' I I I ' ' I I . 30 40

43 50 60 70 7,1

80 85

90 100 110 100

#18211; 2-Heptanone, 7,7-dichloro- 120 130 140 140 _ A— 6.20 m/z 100.05 6.40 6.60 6.80 12.89% 5000 58 J 67 75 103 tM- Tl/Z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

22917.D NP091101.M Wed Oct 03 ll:07;55 2001 Page 1

NYC-WTC_000087594

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NYC-WTC_000087594Source: NYC Law Department, mirrored locally

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