Gas chromatography-mass spectrometry analysis of sample AD24482 completed November 13, 2001, identifying other unknown compounds with violations referenced in comments.
NYC-WTC_000068748–000068762Folder label: “GCMS Scan X 10/15/01 A 11/3/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0 201\24482.D vial: 21 Acq On 3 Nov 2001 10:28 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.54 0.51 ug/1 71517 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3 -Hexanj 102 C6H14O 000623-37-0 78 2 3-Pen mol, 2-methyl- 102 C6H14O 000565-67-3 42 3 Amyl ne Hydrate 88 C5H12O 000075-85-4 36 4 Sil, e, trimethyl- 74 C3H10Si 000993-07-7 33 Abundance Scan 163 (6.543 min): 24482.D (-) m/z 58.95 100.00% 5b
5000 73 43
6.20 6.40 6.60 6.80
■n/z-> ..... Ijlt... . ..... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 85 100 TT-pT-rrp-rrq- m7z 55.00 90.55% Abundance #63527: 3-Hexanol 5b
. 5000 73 31 6.20 6.40 6.60 6.80 m/z 73.00 45.81% 45 84 ... t4 I'''' I -p-TTTyTTTTy ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561: 3-Pentanol, 2-methyl- 5b ...................... 6.20 6.40 6.60 6.80 5000 73 m/z 43.00 35.31% 31 45 .... l'l"l..... 4 85 102 I" " I ‘" 1"'' I"'' I'" ‘ I'' “ I ‘' I' Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62938; Amylene Hydrate ' I ' ' ' ' I 5b _a20_640_6^ 6.80 m/ z 40.95 25.31%
uW' 73 5000 31 43
2£ 11" 111111111 1111111.1 ... 'Ill . ... P' I " '1 ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80
24482.D NP103001.M Fri Nov 09 14:54:33 2001 Page 3
NYC-WTC_000068758
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000068763
Laboratory report documenting GCMS analysis of sample AD24483 identifying unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068529
Laboratory report documenting GCMS analysis of sample AD24480 conducted on November 14, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069587
Laboratory report documenting GCMS analysis of sample AD25377 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068447
Laboratory report documenting GCMS analysis of sample AD24473 conducted on November 9, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068572
Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068585
Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068634
Laboratory report documenting GCMS analysis of sample AD24492 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068893
Laboratory report documenting GCMS analysis of sample AD24730 identifying unknown compounds on November 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067675
DEP lab report for GCMS analysis of sample AD23948 conducted on October 25, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067796
Laboratory report documenting GCMS analysis of sample AD23998 conducted on October 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067752
Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089461
Laboratory report documenting GC/MS analysis of sample AD23833 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000068720
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
Filed in the same folder
NYC-WTC_000068721
Document page containing identification codes for GCMS scans conducted in November 2001 within DEP Box 60.
Filed in the same folder
NYC-WTC_000068724
Instrument data sheet containing operational parameters and sample details for GCMS analysis conducted on October 15, 2001.
Filed in the same folder
NYC-WTC_000068737
Laboratory report documenting GCMS analysis of sample AD24333 with detection of unknown compounds on November 27, 2001.
Filed in the same folder
NYC-WTC_000068763
Laboratory report documenting GCMS analysis of sample AD24483 identifying unknown compounds on November 13, 2001.
Filed in the same folder