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GC/MS analysis results for sample AD23323, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23323 conducted on October 15, 2001.

NYC-WTC_000088290–000088315

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088299
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23323.D Vial: 16 Acq On : 12 Oct 2001 4:47 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.46 ug/1 44667 1,4-Dichlorobenzene-d4 11.76 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hex^ol 102 C6H14O 000623-37-0 83 2 3-Pe^anol 88 C5H12O 000584-02-1 42 3 Amy^ne Hydrate 88 C5H12O 000075-85-4 38 4 3yPentanol, 2-methyl- 102 C6H14O . 000565-67-3 36 ^bund^r<ce Scan 172 (6.622 min): 23323.D (-) m/z 59705 100700% 5b

73

43

84 . JU. 6.20 6.40 6.60 6.80 7.00 i".l|iili| 4+ m/z 55700 78.14% tt/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762: 3-Hexanol 5b

31 5000 43 73 6.20 6.40 6.60 6.80 7.00 “mTz 73700 51.40% 44 I.....'I 102 I'“ ‘I ‘ 'I Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62943:3-Pentanol 5b .... .......... 31 6.20 6.40 6.60 6.80 7.00 5000 m/z 43.00 29.52% 41

.. T-t-l- I'''' I " " I'' " I'''' I jy " I'''' I' I'" ‘ I TiZ2-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62940: Amylene Hydrate 5l9 6.20 6.40 6.60 6.80 7.00 m/z 41.05 19.81% 73 552 45 31

I' ‘' I' I'' I ''' I t+t |""l""|li ' I “ " I'''' I' I"" I " " I " "I" " I' n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80 7.00

23323.D NP091101.M Mon Oct 15 10:29:20 2001 Page 3

NYC-WTC_000088299

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NYC-WTC_000088299Source: NYC Law Department, mirrored locally

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