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GC/MS analysis results for sample AD23323, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23323 conducted on October 15, 2001.

NYC-WTC_000088290–000088315

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088298
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23323.D Vial: 16 Acq On : 12 Oct 2001 4:47 pm Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 6.49 1.00 ug/1 97400 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 2-Hexani .e 100 C6H12O 000591-78-6 91 2 2-Hexi xione, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 2-H Xanone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2I 061141-74-0 59 4 Me .yl Isobutyl Ketone______________ 100 C6H12O 000108-10-1 58 ^bundanbe Scan 158 (6.493 min): 23323.D (-) TmTz 42.95 100.00% 43 (1

58 5000

I-I-p- T 85 100 6.20 6.40 6.60 6.80 ' I ' 1 I ‘ ‘ 71 ' I ' ' ' ' I ' ,1...... ) , ......... ■ . . I I , , , , I , m/z 58.05 57.49% TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 ^bundance #1556:2-Hexanone 43

58 5000 _a20_640__a60__a80^_ m/z 41.05 17723% 27 ' ' I I, ■ ..,.1 ■ •n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance • -43 #11968; 2-Hexanone, 4-hydroxy-3-propyl- /vaJvUJV 58 6.20 6.40 6.60 6.80 5000 29 ■m/z 57.00 16.13%

100 ^1--- 1 I J. ' I ' ' ' ' I ' ' ' ' I ’ 71 I 85 T-p-rS- ............. ........................................ I . . 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #15807: 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 4)3 _a2g_6;4g__6;6g__&BgL^_ m/z 100.05 11.23% 5000 58 27

Tl/Z-> -UL ' I ' ‘ * 'I ' 20 30 40 -t-rn-p 50 1 ................................ 60 70 72

80 90 100 110 120 130 140 A 6.20 y 6.40 6.60 6.80

23323.D NP091101.M Mon Oct 15 10:29:17 2001 Page 2

NYC-WTC_000088298

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NYC-WTC_000088298Source: NYC Law Department, mirrored locally

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