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GC/MS analysis results for sample AD23323, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23323 conducted on October 15, 2001.

NYC-WTC_000088290–000088315

Folder label: “GC/MS Scan 9/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\OCT1201\23323.D vial: 16 Acq On : 12 Oct 2001 4:47 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.46 ug/1 45344 1,4-Dichlorobenzene-d4 11.76 Hit# of Tentative ID MW MolForm CAS# Qual

1 3-He^none 100 C6H12O 000589-38-8 91 2 But^e, 2,2-dimethyl- 86 C6H14 000075-83-2 59 3 3-^ntanone, 2-methyl- 100 C6H12O 000565-69-5 47 4 q^ane, 3,3,4- trimethyl-_________ 128 C9H20 016747-31-2 45 Abundance Scan 146 (6.383 min): 23323.D (-) m/z 4^760 iWTcm. 43 57

71 5000 100 6.00 6.20 6.40 6.60 6,80 85 I" " I" " I" “ I tpTTTT^ . .... . I ’"' 1’ I" " I m/z SYTOO 82.45% Ti/z-> 5 10 15 20 25 30 35 40 45 50'55 60 65 70 75 80 85 90 95 100105 Abundance #1528: 3-Hexanone 57

29 71 7 5000 6.00 6.20 6,40 6.60 6.80 100 m/z 71.00 62.05%

7 'I........... I' 'r r I I"......... I Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #732: Butane, 2,2-dimethyl- 43' 5|7 71 6.00 6.20 6.40 6.60 6.80 29 m/z 100.05 28.21% 5000

15 pTrT|Tm I -tpriTrn+T irpTTri^ I" I" " I" " I" " I" " I"" I" " I" " I ttZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63398: 3-Pentanone, 2-methyl- ' a..... 5)7 6.00 6.20 6.40 6.60 6.80 43 "mTz 41.05 22.15% 5000 100 71 85 tTTrprrrTT -n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

23323.D NP091101.M Mon Oct 15 10:29:15 2001 Page 1

NYC-WTC_000088297

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NYC-WTC_000088297Source: NYC Law Department, mirrored locally

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