GC/MS analysis report for sample AD22545, September 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\l\DATA\SEP2501\22545.D Vial: 11 Acq On : 26 Sep 2001 12:15 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NPO91101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.39 0.42 ug/1 51276 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual 1 3-Hexanone 100 C6H12O 000589-38-8 90 2 Butarie, 2,2-dimethyl- 86 C6H14 000075-83-2 38 3 3-^ntanone, 2-methyl- 100 C6H12O 000565-69-5 38 4 Bi/tane, 2-methyl- 72 C5H12 000078-78-4 35 ^bundc/ice Scan 147 (6.388 min): 22545.D (-) m/z 43.05 100.00% 4(3 57 71 5000 100 6.00 6.20 6.40 ^60 6.^ (" " r'"I m/z 57.00 78717% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63358: 3-Hexanone 4(3 57

71 --- --- 5000 6.00 6.20 6.40 6.60 6.80 100 m/z 71.00 61.82% I"" I J 85 ■I............ II"'' I ■nfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance

JUMw- #732: Butane, 2,2-dimethyl- 43 5|7 71 6.00 6.20 6.40 6.60 6.80 29 m/z 100.05 33.33% 5000

15 +rTTrTTTT+TT■ '.... I" I"" I' I"" I"" I"" I"" I""I Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63398:3-Penfanone, 2-methyl- 5(7 6.00 6.20 6.40 6.60 6.80 43 m/z 41.05 25.40% 5000- 100 71

I" " r' ‘' I" " I"'' I L 85 I" " I"'' I" " I" " I T' '"I Tl/Z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

22545.D NP091101.M Wed Oct 03 15:09:27 2001 Page 1

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