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GC/MS analysis results for sample AD22773, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22773 conducted on October 11, 2001, noting other unknown compounds.

NYC-WTC_000087417–000087432

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22773 .D Vial: 20 Acq On : 29 Sep 2001 7:04 am Operator; 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.38 0. ug/1 53338 1,4-Dichlorobenzene-d4 11.78 Hit# of Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H12O 000589-38-8 91 2 3-Pentanone, 2-methyl- 100 C6H12O 000565-69-5 38 3 Butane, 2,2-dimethyl- 86 C6H14 000075-83-2 36 4 2Pentanedione _________________ 100 C5H8O2 000123-54-6 35 Abundant Scan 146 (6.378 min): 22773.D (-) Wz 43.05 100.00% 4(3 57 71 5000 100

6.00 a20_a4o__a60L_6^ I" " I t I" " I I" " I m/^ 57.00 80.74% v/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1528: 3-Hexanone '’(3 57

29 71 5000- 6.00 6.20 6.40 6.60 6.80 100 m/^ 71.00 57.18% A tW ....... ...... ..... TiZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63398; 3-Pentanone, 2-methyl- 5|7 43 6.00 6.20 6.40 6.60 6.80 5000 m/z 100.05 32.50% 100 71 85 I ' I" " I I......... ..... T!^->51O152O 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 A A, , , ,/ Abundance #732: Butane, 2,2-dimethyl- 43 5|7 6.00 6.20 6.40 6.^ 6.80 71 “mTz 41.05 24.94% 29 5000

... Y , Tl/Z-> 5_IO152O^3O 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

22773.D NP091101.M Fri Oct 05 14:23:49 2001 Page 1

NYC-WTC_000087428

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NYC-WTC_000087428Source: NYC Law Department, mirrored locally

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