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GCMS analysis results for sample AD23997, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23997 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067782–000067795

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\23997.D Vial: 5 Acq On : 25 Oct 2001 4:36 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.35 0.43 ug/1 85065 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone / 100 C6H12O 000589-38-8 91 2 3-Heptanone, A-methyl- 128 C8H16O 006137-11-7 42 3 3-Pentanone< 2-methyl- 100 C6H12O 000565-69-5 38 4 Butane, 2, -dimethyl- 86 C6H14 000075-83-2 36 Abundance Scan 143 (6.355 min): 23997,0 (-) Wz 43.00 100.00% 43 57

71 5000 100 T 600 6.20 6.40 6.60 51 , m/z 57.00 85.64% ' ' • i'''' ' +1^ n/z-> 20 30 40 50 70 80 90 100 110 120 W <\bundanc8 #1528:3-Hexanone 43 57

29 71 5000 Roo' 'e.^' 'e.^' ''' 100 m/z 71.00 55.18% h-p-r+Mj-r •nZz-> 20 30 50 60 70 80 90 Btbunebnea #5035:3-Heptanon8,4-m8thyl- 43 5|7 29 71 6 00 6.20 6.40 6.60 5000 m/z 100.05 35.02% 86

99 128 t.p.J.I,.....J iiZz-> 20 30 40 50 60 70 80 90 100 iioZjMZZiH Abundance #63398:3-Pentanone, 2-methyl- I 1 J . I i I I I I f < p 1 f I I f 1 « I I I

6.00 620 6.40 6.60 43 m/z 41.05 23.11% ft 5000 1C» 71

,1, 85 m/z-> 20 30 40 50 60 70 80 90 100 110 ioO ' 6.^ 6.^ 6.^ 1M130

23997.D NP101901.M Fri Oct 26 10:10:55 2001 Page 1

NYC-WTC_000067790

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NYC-WTC_000067790Source: NYC Law Department, mirrored locally

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