GCMS analysis results for sample AD25457, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1401\25377.D Vial: 12 Acq On : 15 Nov 2001 3:20 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.33 0.45 ug/1 75248 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone Z 100 C6H12O 000589-38-8 86 2 3-Pentanon^ 2-methyl- 100 C6H12O 000565-69-5 46 3 Hexane, 2z<4,4- trimethyl - 128 C9H20 016747-30-1 36 4 Heptane,^! , 3-dimethyl- 128 C9H20 004032-86-4 33 Abundance Scan 140 (6.328 min): 25377.D {-) m/z 43.00 100.00% 4l3 57

71 5000

85 100

6.00 6.20 AJ 6.40 6.60 , 49 , m/z 57.00 92.72% 4^ Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #63358:3-Hexanone 43 57

71 5000 6.00 6.20 6.40 6.60 100 m/z 71.00 56.94% 85 - +t " I" " I I' " ' I' " ’ I ""I mZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #63398: 3-Pentanone, 2-methyl- 5(7 43 6W620 6.40 6.60 5000 m/z 100.0^ 37.14% 100 71

Ti/z-> Abundance r " 'I'" 'I' 85 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120

4(3 #65107: Hexane, 2,4,4-trimethyl- 5(7 71 I , . I . I . I I , I 1 ■ I . 1 1 . I . I V. I 6.00 "m/z 6.20 41.05 6.40 6.60 19.44% 5000

27 99 83 I113 Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 6.00 6.20 6.40 6.60

25377.D NP103001.M Wed Nov 21 12:57:07 2001 Page 1

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