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GCMS analysis results for sample AD25457, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25457 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069601–000069613

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1401\25377.D Vial: 12 Acq On : 15 Nov 2001 3:20 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L 11;****************************************************************'*"*** Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.84 ug/1 139711 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone X 100 C6H12O 000591-78-6 91 2 Oxirane, 2 iethyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 80 3 2-Hexano , 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4 2-Hexa^me, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 59 Abundance Scan 151 (6.429 min): 25377.D (-) m/z 42.95 100.00% 4P

58 aiBB!

7. 85 100 207 6.00 6.20 AJ 6.40 6.60 6.80 -TT—- .. 1... \.... "mTz 58705 57.69% TTfe-> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance #1556: 2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 “m/z 57.00 17.12% 27 71 85 1(^ ' I'''' I' "'I'' " I' " ' I • " ' I I'' " I " ' ‘ I 1' " ' I " ' ‘ [ 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 43 58 6.00 6.20 6.40 6,60 6.80 5000 Wz’ 41705 15.15% 71

30 85 100 ..... .......... I"'.. I.. .... I" " I" " I" ' 1" " I' *" I" " 1 ■n/z-> :20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance! #11968: 2-Hexanone, 4-hydroxy-3-propyl- 413 6,00 6,20 6.40 6.60 6.80 Wz 85.05 10.08% 58

5000 29

71 85 I00 140 " I' "' I I " ‘' I " " I —y-r-T—TT—p— n/z-> 20 30 40 50 60 70 80 90 100110 120130140150160170180190 200 210 6.00 6.20 6.40 6.60 6.80

25377.D NP103001.M Wed Nov 21 12:57:09 2001 Page 2

NYC-WTC_000069610

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NYC-WTC_000069610Source: NYC Law Department, mirrored locally

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