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GCMS analysis results for sample AD25457, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25457 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069601–000069613

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV1401\25377.D Vial: 12 Acq On : 15 Nov 2001 3:20 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

6.68 0.44 ug/1 73244 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexano]^ 102 C6H14O 000626-93-7 78 2 2-Pentan<n, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-Octazfol, (.+/-.)- 130 C8H18O 004128-31-8 56 4 2-Heptanol, (S) -______________________ 116 C7H16O 006033-23-4 39 Abundance » Scan 178 (6.677 min): 25377.D (-) m/z 44795 100.00% 4)5 1

.......w II.. r I I . I , , I i~)”i 1 1 1 69 5lji^ || ■ 98 6.40 6.60 6.80 7.00 “m/z 41.05 17700% 'Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63584: 2-Hexanol 45

5000 6.40 6.60 6,80 7.00 69 m/z 69.10 14.00% 19 27 - 56 I 87 •n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1773: 2-Pentanol, 4-methyl- 4^ AA f' 6.40 6.60 6.80 7,00 5000 m/z 43.00 12.54%

27 69 57 ................. Ji|ii.,||l| 71/Z-> 10 20 30 40 50 60 70^80^ 90 100 110 120 JJ

u ^bundance #5517; 2-Octanol, (.+/-.)- 4 6.40 6.60 6.80 7.00 m/z 44.00 9.42%

5000

5,7 69 84 97 ns ' I I ' I'l I , , , I'l , , , I I .1 ■ , I , , ,'i I . , I , I , , , I I , ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 6.40 6.60 6.80 7.00

25377.D NP103001.M Wed Nov 21 12:57:10 2001 Page 3

NYC-WTC_000069611

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NYC-WTC_000069611Source: NYC Law Department, mirrored locally

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