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GCMS analysis results for sample AD24046, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD24046 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067811–000067825

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT2501\24046.D Vial: 7 Acq On : 25 Oct 2001 6:33 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Libranry : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.71 0.55 ug/1 102079 l,4-Dichlorobenzene-d4 11.74 Hit# Of 5 'entative ID MW MolForm CAS# Qual 1 2-Hexanoy 102 C6H14O 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 64 3 2-Octaifol, (R)- 130 C8H18O 005978-70-1 40 4 2-Octgnol, (.+/-.)-_________________ 130 C8H18O 004128-31-8 40 Abundance Scan 181 (6.708 min): 24046.D (-) m/z 44795 100.00% 4)5

5000

, . . )T . I , I . . 69 51.^ ' I "'''I ■ I ' I , ' { ' * ‘ ' 1 ‘ 101 ’ 1 ' ‘ ‘ T’ • ' ' I ’ m/z 6.40 6.60 69.00 6.80 7.00 15.80% TiZz-> 10 20 30 40 50 60 TO 80 90 100 110 120 Abundance #63582:2-Hexanol 45

5000 , ......... AI 6.40 6.60 6.80 7.00 27 m/z 41.00 11711% 69 19 I . ..I,......................... -......... TiZz-> 10 20 30 40 50 60 70 80 90 too 110 120 Abundance #63545:2-Pentanol. 4-melhyl- 4|5 6.40 6.60 6.80 7.00 ' 5000 ■m7F~4J795^ 10.88%

69 ......... 57 I 87 ) ,l, , , , , , ......... Tife-> 10 20 30 40 50 60 70 80 90 too 110 120

u ^bundance #5523:2-Octanol, (R)- 45 6.40 6.60 6,80 7.00 m/z 44.00 10.67% 5000

27 57 69 84 97 115 V--' . I.. 7'. I ■... 111 p ' - p " ''h mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 6.40 6.60 6.80 7.00

24046.D NP101901.M Fri Oct 26 12:20:31 2001 Page 4

NYC-WTC_000067822

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NYC-WTC_000067822Source: NYC Law Department, mirrored locally

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