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GCMS analysis results for sample AD25377, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25377 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069587–000069600

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1401\25376.D Vial: 11 Acq On : 15 Nov 2001 2:22 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.55 0.64 ug/1 104300 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanoy 102 C6H14O 000623-37-0 83 2 3-Pentahol, 2-methyl- 102 C6H14O 000565-67-3 39 3 3-Pent^ol 88 C5H12O 000584-02-1 38 4 1,2-Butanediol, (.+/-.)- 90 C4H10O2 026171-83-5 36 Abundance * Scan 164 (6.548 min): 25376.D (-) m/z 59700 100.00% 50 li 5000 73 41 ...... ................. 51 6.20 6.40 6.60 6.80 85 - lllll...... m/z 54795 83.85% 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529: 3-Hexanol

31 . . (TV.. I ... I I .... I . 5000 73 6.20 6.40 6.60 6.80 m/z 73.00 44.41% 44 ...... ... 102 I- tt/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561: 3-Pentanol, 2-methyl-

620 6,40 6.60 6,80 5000 73 “mTz 41.05 31.29% 31 45 85 I""I""I 4 102 Tp-TTTyT-nn-p-ri-q-TTTTpnT-rpnn-rp-rT^^ mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62943:3-Pentanol 50 620 6.40 6.60 6.80 m/z” 42.95 25.28% 31 5000

41

...... I"'' I'"' I ‘" I'''' I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80

25376.D NP103001.M Wed Nov 21 12:56:17 2001 Page 3

NYC-WTC_000069597

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NYC-WTC_000069597Source: NYC Law Department, mirrored locally

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