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GCMS analysis results for sample AD25377, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25377 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069587–000069600

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV1401\25376.D Vial: 11 Acq On : 15 Nov 2001 2:22 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.85 ug/1 138486 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexan 102 C6H14O 000626-93-7 83 2 2-Pent .ol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-Oct Aoi, (S)- 130 C8H18O 006169-06-8 64 4 2-He: nol, 3-methy1- 116 C7H16O 002313-65-7 64 Abundance Scan 177 (6.668 min): 25376.D (-) m/z 44.95 100.00% 4(5

5000

69 T-T-p-r-r-r-p-r-r-' * 55 6.40 6.60 6.80 7.00

m/z-> I ' ' ' ' I ' ' 10 20 30 40 p-^4vp 50 60 470 80 90 ............................. 100 110 120 m/z 69.00I 14.46% Abundance #63584: 2-Hexanol 45

u '-A 6.40 6.60 6.80 7.00 69 m/z :44.00 12.00% 19 27 56 I 87 AtA- rnfe:^>^^IO^O^O^ 50 60 70 80 90 100 110 120 Abundance #63546:2-Pentanol. 4-melhyl- 45

6.40 6.60 6.80 7.00 5000 m/z 41.00 11.96%

27 19 ■I.......... . 57 ......y................ mZz-> 10 20 30 40 50 60 70 80 90 100 110 1^ Abundance #5558: 2-Octanol, (S)- 45 6.40I 6.60 6.80 7.00 m/z 43.00 11.84%

L ass 27 56 ...............................ill m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 6.40 6.60 6.80 7.00

25376.D NP103001.M Wed Nov 21 12:56:18 2001 Page 4

NYC-WTC_000069598

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NYC-WTC_000069598Source: NYC Law Department, mirrored locally

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