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GCMS analysis results for sample AD25377, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25377 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069587–000069600

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1401\25376 .D Vial: 11 Acq On : 15 Nov 2001 2:22 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 5.85 ug/1 947541 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 2-Propan/l, 2-methyl- 74 C4H10O 000075-65-0 17 3 Acetone/ 58 C3H6O 000067-64-1 10 4 Morpho/ine, 4-methyl- 101 C5H11NO 000109-02-4 9 /Xbundance Scan 287 (7.678 min): 25376.D (-) m/z 42795 100.00% 4b

59 5000

101 7.40 7.60 7.80 8.00 69 +T I"'' I"'' I" " I m7z 59.05 51717% rnfe-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 413

lililil 59 7.40 7.60 7.80 8,00 m/z 100.95 21.73% 27 101 83 I" I' 11." I" . 11 I.............. Tife-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #62572: 2-Propanol, 2-methyl- 5b

7.40 7.60 7.80 8.00 5000 m/z 58.05 17.60% 31 41

"I *li-|"i,|i"i|ll, % I " " I " ” I " " 1 " " I I ' H I H 1 I I I. " I " " I" " I I I I I I ■ I I tVz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Sundance #62322: Acetone 43 7.40 7.60 7.80 8.00 m/z 41.05 7.59% 5000 58 27 ^^rTTtjlrHTTTTTrrr+T# I'' " I " " I hTfe-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 7.40 7.60 7.80 8.00

25376.D NP103001.M Wed Nov 21 12:56:20 2001 Page 5

NYC-WTC_000069599

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NYC-WTC_000069599Source: NYC Law Department, mirrored locally

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