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← Document results/DEP Box 60/508 GCMS Scan X 10/11/01 An 11/2/01
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GCMS analysis results for sample AD24398, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD24398 with detection of unknown compounds.

NYC-WTC_000068303–000068313

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068311
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24398.D Vial: 4 Acq On : 2 Nov 2001 5:58 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.02 ug/1 153902 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentano:n^ 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 3-Hydro; ^2-pentanone 102 C5H10O2 003142-66-3 23 3 AcetamLde 59 C2H5N0 000060-35-5 9 4 Morphgl ine, 4-methyl- 101 C5H11NO 000109-02-4 9 Abundance / Scan 289 (7.694 min): 24398.D (-) m/z 4^790 100.00% 4)3

59 5000

101 7.40 7.60 7.80 8.00 83 I‘‘‘1‘‘‘'I‘' 1'' ' 11 ‘ ' I m/z 59.05 52.11% mfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone. 4-hydroxy-4-methy^ 4(3

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 20.61% 27 101 I I 83 ' ' ' I mfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance

5000 3h #1691:3-Hydroxy-2-pentanone 59

m/z 7.40 1... 7.60 58.05 7.80 8.00 18.69% 45 15 , ' I ' I...... II...... I I • ' I ‘ • • • |“r“r rr ( 1 l| . 1 A ■ , , ■ ■ ■

m&-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #103: Acetamide 44 5|9 ' '7.46 Teo 7.80 8.00 m/z 40.95! 7.53% 5000

26 31 3^1 —J—n—T-j—j—1 ‘ 1 ' ‘ ‘ ' 1 ' ' ' ' I ' ' ' ' I ' ' ' ' I ‘ ‘ I ' ‘ ‘ ‘ I 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

24398.D NP103001.M Mon Nov 05 12:18:41 2001 Page 1

NYC-WTC_000068311

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NYC-WTC_000068311Source: NYC Law Department, mirrored locally

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