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GCMS analysis results, sample AD25461, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25461 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069659–000069675

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV1601\25461.D Vial: 3 Acq On : 16 Nov 2001 4:59 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.70 1.28 ug/1 220564 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolFoirm CAS# Qual

1 2-Pentanoni 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 38 2 3 Hydroxy-, pentanone 102 C5H10O2 003142-66-3 9 3 Acetone / 58 C3H6O 000067-64-1 9 4 Morpholipfe -methyl- 101 C5H11NO 000109-02-4 9 Abundance Scan 289 (7.701 min): 25461 .D (-) m/z 4 2'. 9 5 100.00% 4(3

59 5000

101 7.40 7.60 7.80 8.00 83 Ml ' 'I +-r-r-p 4 I ' ' ' ' I ' ' ' ' I ' I ' ' ' I I I ' ' ' I 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Penlanone, 4-hydroxy-4-methyl- 4(3

5000 59 _7;40__Y60__7,80__a00__ m/z 101.05 227740% 101

L 15 31 83 ................ ' 1 ' I ' ‘ ' I ' ' ' ' 1 ' ' ' ' p m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 3|1 59

7.40 7,60 7.80 8.00 5000 m/z 58.05 17.68% 45 15 1 ■ I /? . . I . I . ■ . . ■ . I 1—I—]—r-r-r-r-|-r-r-r-r-p mfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone 43 7.40 7.60 7.80 8.00 “mTz 41.05 7731%

5000 58 27

50 60 70 80 '^100 110 7.40 7.60 7.80 8.00 ■ntz-> 10 20 30 40

25461.D NP103001.M Wed Nov 21 11:43:22 2001 Page 1

NYC-WTC_000069667

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NYC-WTC_000069667Source: NYC Law Department, mirrored locally

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