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← Document results/DEP Box 60/508 GCMS Scan X 10/11/01 An 11/2/01
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GCMS analysis results for sample AD24398, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD24398 with detection of unknown compounds.

NYC-WTC_000068303–000068313

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068312
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C!\HPCHEM\1\DATA\NOV0201\24398.D Vial: 4 Acq On : 2 Nov 2001 5:58 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.51 ug/1 77203 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlordbenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-1,2<3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 56 3 Benzenamine, N-methyl-4-nitro- 152 C7H8N2O2I 000100-15-2 14 4 2-Adamantanone 150 C10H14O 000700-58-3 9 Abundance Scan 712 (11.577 min); 24398.D (-) m/z 149.90 100.00% It®

5000 115

52 78 ' ‘' r 1120 11.40 11.60 11.80 12.00

Tife-> 20 " I' ■ "'I 30 38 45 40 ■ 50 60 87 ' ”‘i' A 70 80 90 100 110 120 130 140 150 160 I'''' I m/z 151.90 67.69% Wjundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 J T ' ‘ 11.20 11.40 11.60 11.80 12,00 52 78 m/z 114.90 . 44.06% 35 • I' ‘ ' 1 • " ' 1 ’''' I' T I'''' I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro liO

11 5 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78705^ 13716%

35 87

iVz-> 20 30 I 40 50 ■ 1''' ' I' ' 60 70 I 11 ■ ■ ■ ■ I ■ A 80 90 100 110 120 130 140 150 160 Abundance #10120: Benzenamine, N-methyl-4-nitro- T T 1!2 11.20 11.40 11,60 11.80 12.00 m/z 116.95 14.52% 77 122 110 5000 65 30 .. 1. 1.5^, I... 11.1 ' I I I ■ ■ ■ 1 • ■ ■ ■ I TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24398.D NP103001.M Mon Nov 05 12:18:43 2001 Page 2

NYC-WTC_000068312

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NYC-WTC_000068312Source: NYC Law Department, mirrored locally

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