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GCMS analysis results, sample AD23900, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23900 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067453–000067466

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\OCT1701\23900.D Vial: 5 Acq On : 17 Oct 2001 5:12 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C!\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.52 ug/1 46468 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 50 2 Benzenamiiib; 2-methyl-4-nitro- 152 C7H8N2O2I 000099-52-5 12 3 Benzenanuzne, 2-methyl-5-nitro- 152 C7H8N2O2i 000099-55-8 10 4 Benzeiip^,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 9 <\bundance Scan 718 (11.629 min): 23900.D (-) m/z 149.90 100.00% 1$0

5000 115 52 78 11.20 11.40 11.60 11.80 12.00 40 I I' "'I''' 1 ‘ ' I ' I ' ' ' ' I ....... m/z 151.90 65.88% nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 IK) Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 36.41% 35 87 1 ' I '' ‘' I' nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyI-4-nitro- 77 106 1ii2 f-ryp 11.20 11.40 11,60 11,80 12.00 5000 m/z78.05 19.71% 51 94 66 ' KJ '' 70 '' '' I' ' I'' ‘ ‘ I'''' I ‘ ‘' I ‘‘' I nZz-> ' 30 " "40" ' '50' 100 110 120 130 140 150 IK) '' I '

Abundance #66885: Benzenamine, 2-methyl-5-nitro- 77 106 152 11.20 11.40 11.60 11.80 12.00 ■m/z 52.00 16.89%

5000 51 94

66 ' I ' ' '' 1 ' ' '' I • ' ' ' I' mZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11,80 12.00

23900.D NP101901.M Tue Oct 23 12:46:20 2001 Page 5

NYC-WTC_000067465

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NYC-WTC_000067465Source: NYC Law Department, mirrored locally

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