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GCMS analysis results, sample AD23910, Oct 2001

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Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

NYC-WTC_000067579–000067600

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23910.D Vial: 5 Acq On : 18 Oct 2001 8:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.53 ug/1 47791 1,4-Dichlorobenzene-d4 11.76 Hit# Of 5 Tentatj.ve ID MW MolForm CAS# Qual 1 1,4-Dichlorobprizene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2x374-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 28 3 Benzenamine, 2-methyl-4-nitro- 152 C7H8N2O2! 000099-52-5 14 4 Benzenajgine, 2-methyl-5-nitro- 152 C7H8N2O2i 000099-55-8 14 ^bundance Scan 717 (11,627 min): 23910,D (-) m/z 149.90 100.00% 1$0

5000 115 52 78 T 40 11,20 11.40 U.K) 11,80 12,00 I" I'"til I m/z 151.90 67717% TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 liB

5000 115 78 11,20 11,40 11,60 11,80 12,00 52 m/z 114.90 . 34.78%

Tife-> 30 35 40 50 „,.ll,..?..........1,1.......... 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2.3,4-d4-, 5,6-dichIoro- 1!i0 1^' ' ' I 115 11,20 11,40 11,60 11,80 12,00 5000 52 78 "m/z 78.05 . 22.41%

35 87

nfe-> 30 I 40 1 ■ 11 ■ ■ ■ 1' ■'' I ‘' I' I'''' I ‘ 50 60 70 80 90 100 110 120 130 140 150 160 -rJJn- Abundance #10129: Benzenamine, 2-methyl-4-nitro- 77 106 1512 11,20 11,40 11,60 11,80 12,00 ■m/z 75.90 , 18.98%

5000 51 94 66 nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11,20 11,40 11,60 11,80 12,00

23910.D NP091101.M Fri Oct 19 10:18:08 2001 Page 5

NYC-WTC_000067591

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NYC-WTC_000067591Source: NYC Law Department, mirrored locally

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