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GC/MS analysis results for sample AD23341, Oct 19 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23341 conducted on October 19, 2001.

NYC-WTC_000088648–000088659

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088658
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1801\23341.D Vial: 9 Acq On : 19 Oct 2001 12:01 am Operator: 209 GALOS Sample : gc/ms unknown re extracted Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.51 ug/1 47721 1,4-Dichlorobenzene-d4 11.76 Hit# Of 5 Tentdtive ID MW MolForm CAS# Qua! 1 1,4-DichlorQbenzene-d4 150 C6C12D4 003855-82-1 64 2 Benzene-1 ,^3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 32 3 Benzenam^e, 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 22 4 Benzenaijtlne, 2-methyl-5-nitro- 152 C7H8N2O2 _____ 000099-55-8 14 flibundance Scan 718 (11.629 min): 23341.D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 11.20 11.40 11.60 11.80 12.00 40 I Tife-> 30 ‘ ' I ' ' ‘ 'I''. ' ' 1 . i 40 50 ' I' 60 70 80 90 ... IK. I. 100 110 120 130 140 150 160 m/z 151.90 67721% Abundance #9593:1,4-Dichlorobenzene-d4 1'10

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 38.98%

■il/z-> 30 35 40 50 ........ II,..?,. 100 110 120 130 140 150 160 60 70 80 90 ^bundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 11.20 11,40 11.60 11.80 12.00 5000- 52 78 m/z 78.05 20.91%

87

Jk 35 I I ' I'''' I' ' I ' ' ' ' I ' ' ' ' I ' iife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- 77 1Q6 152 11.20 11.40 11.60 11.80 12.00 “mTz 52.00 17.29%

5000 51 94 66 ' I ' ' '' I ' ' ' ' I ' I ' ' ' ' I ' ' ' ‘ I ' Tlfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23341.D NP091101.M Fri Oct 19 10:12:52 2001 Page 3

NYC-WTC_000088658

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NYC-WTC_000088658Source: NYC Law Department, mirrored locally

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