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GC/MS analysis results for sample AD23325, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23325 conducted on October 16, 2001.

NYC-WTC_000088504–000088519

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088518
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23325.D Vial: 12 Acq On : 10 Oct 2001; 12:06 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.53 ug/1 56468 1,4-Dichlorobenzene-d4 11.75 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlbrobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene/1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 38 3 Benzen, (mine, 2-methyl-4-nitro- 152 C7H8N2O2: 000099-52-5 22 4 Benzene imine, 2-methyl-5-nitro- 152 C7H8N2O2i _____ 000099-55-8 14 Abundance / Scan 716 (11.617 min): 23325.D (-) m/z 149.90 100.00% I'iO

5000 115 52 78 40 11.20 11.40 11.60 11.80 12.00

Ti/z-> '' I''' I'h'' 30 40 50 60 70 80 90 rX 100 110 120 130 140 150 160 m/z 151.90 62.22% ^bundance #9593: 1,4-Dichlorobenzene-d4 1!i0

5000 115 ... 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 33.95% 35 ... 1,1... II Tife-> 30 40 50 60 70 80 100 110 120 130 90 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0

115 11.y 11.40 11.60 11.80 12.00 5000- 52 78 m/z 77.95 19.56%

35 87 1 ' I ' ' ' ' I ‘ I 44^ ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- 77 106 152 11.20 11.40 11.60 11.80 12.00 m/z 52.00 16.12%

5000 51 94 66 ' ' r ' ' ‘ I ' I *' • ' I ' '' ' I '' ' ' I' ' ' ’ I '' r -P m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23325.D NP091101.M Thu Oct 11 12:57:23 2001 Page 7

NYC-WTC_000088518

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NYC-WTC_000088518Source: NYC Law Department, mirrored locally

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