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GCMS analysis results, sample AD23906, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23906 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067535–000067554

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\OCT1801\23906.D Vial: 3 Acq On : 18 Oct 2001 6:08 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.54 ug/1 55626 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-DichlorQbenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1 ,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 28 3 Benzenarai:.ne, 2-methyl-4-nitro- 152 C7H8N2O2i 000099-52-5 22 4 Benzei^^ine, 2-methyl-5-nitro­ 152 C7H8N2O2i ____ 000099-55-8 22 Abundance / Scan 717 (11.623 min); 23906.D (-) m/z 149.90 100.00% 1!i0

5000 115

52 11.20 11.40 11.60 11.80 12.00 40 87 I yn-r-rttr-r T m/z 151.90 . 64.56% Ttfe-> 30 40 50 60 70 80 90 100 110 140 150 160 Abundance #9593; 1,4-Dichlorob8nzene-d4 1ii0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 38.03% 35 ' I ''' I'' ‘ ‘ I' I ‘‘ ‘ I'''' I ‘ Tife-> 30 " 40’ 50 60 70 80 90 100 110 120 130140 150 160 Abundance #9592: Benzene-1.2,3,4-d4-. 5,6-dichloro- 1$0

115 lljp 11.40 11.60 11.80 12.00 5000 52 78 ■m/z 77795 21.47%

35 87 I T I ‘ ‘ I' T)fe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenatnine, 2-methyl-4-nitro- T 77 106 1il2 11.^ 11.40 11.60 11.80 12.00 “m/z 52.00 15.16%

5000 51 94 66 ■p-n-rT-m-r-j- 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11,80 12.00

23906.D NP091101.M Fri Oct 19 10:16:08 2001 Page 4

NYC-WTC_000067546

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NYC-WTC_000067546Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AD23910, Oct 2001 · Box DEP Box 60

NYC-WTC_000067579

Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

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