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GCMS analysis results, sample AD23906, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23906 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067535–000067554

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23906.D Vial: 3 Acq On : 18 Oct 2001 6:08 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.54 ug/1 55626 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichloroben^ne-d4 150 C6C12D4 003855-82-1 53 2 Benzene -1,2,3z<4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 28 3 Benzenamine< 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 22 4 Benzenamlp^, 2-methyl-5-nitro- 152 C7H8N2O2 000099-55-8 22 Abundance 7 Scan 717 (11.623 min): 23906.D (-) m/z 149.90 100.00% i$o

5000 115

52 78 I ' ' ' ■ I ' 11.M 11.40 11.60 11.80 12.00

nfe~> ........ 30 40 50 60 uLsp 70 80 I 90 100 110 120 130 140 150 160 m/z 151.90 64.56% ‘\bundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 T-T-r(-r ‘ ’ I ' ' 78 11.M 11.40 11.60 11.80 12.00 52 m/z 114.90 38.03%

T)Zz-> 30 35 40 ‘ 1 ‘ ‘ 50 ’ 1 ’ 3. 60 70 80 90 100 110 120 130 140 150 160 I ' ' ' ' I 114^ Abundance #9592: Benzene-1,2.3,4-d4-, 5,6-<iichloro- liiO

115 11.M 11.40 11.60 11.80 12.00 5000 52 78 “m/z 77795 21.47%

35 I 'I' '' ’ P nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 lai 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- ... 77 1Q6 1!i2 11.M 11.40 11.60 11.80 12.00 “m/z 52.00 15.16% 5000 A 51 94 66 —I . . . . I . . . . p-. /, . I . .

nfe-> 30 40 M I 100 110 IM W 140 IM iro 60 70 80 90 1190 1140 11 m 11 RO 1900

23906.D NP101901.M Tue Oct 23 14:31:15 2001 Page 4

NYC-WTC_000067553

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NYC-WTC_000067553Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AD23910, Oct 2001 · Box DEP Box 60

NYC-WTC_000067579

Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

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