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GCMS analysis results for sample AD24732, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24732 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068919–000068930

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24732.D Vial: 6 Acq On : 6 Nov 2001 5:41 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.54 ug/1 99141 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 56 2 Benzene-3^, 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 3 Benzen^ine, 2-methyl-5-nitro- 152 C7H8N2O21 000099-55-8 10 4 Benz§^ldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Abundance Scan 711 (11.575 min): 24732,0 (-) m/z 149.90 100.00%! 1$0

5000 115 I 11M 1L4o' 11.CT 1180 12:00 An 87 1 ‘ I ' ’ ’ * 1 ' ' ‘ ’ I ’ ' ' ' I ’ ' ’ ’ I ’ ‘ ’ 1 * ‘ m/z 151.90 64770% nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593; 1,4-Dichlorobenzene<l4 1$0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 . 35.73%

Tife-> 30 35 40 ,,l....... II,..... 110 50 60 70 80 90 100 120 130 1 ‘ ’ I 140 150 160 Abundance #9592; Benzene-1,2.3,4^4-, 5,6-<iichloro- 1$0 fY t 115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 18.66%

35 87 mtz-> I "30 " '40''' '50 ro 1 ‘ I' ’'' I'' •' (' 70 80 90 100 110 120 130 r-JJn 140 150 160 Abundance #10131: Benzenamine, 2-methyl-5-nitro- , I.... I ,,,:-[ 1 I , .7,1 1 1 I I 1$2 11.20 11.40 11.60 11.80 12.00 77 m/z 52.00 , 13.79% 106

5000-

51

TiZz-> 30 40 50 60 70 80 u 90 94 122 100 110 120 130 140 150 160 I • ■ > ■ 1 • ■ • ■ I 11.20 11.40 11.60 11.80 12.00 T

24732.D NP103001.M Mon Nov 19 10:48:37 2001 Page 3

NYC-WTC_000068929

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NYC-WTC_000068929Source: NYC Law Department, mirrored locally

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