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GCMS analysis results for sample AD25040, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25040 conducted on November 19, 2001, noting violations and unknown compounds.

NYC-WTC_000069245–000069255

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\NOV0801\25040.D Vial: 14 Acq On : 9 Nov 2001 3:18 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.52 ug/1 105486 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichloroben^ne-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1,2,3,^d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 Benzenamine, y-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 12 4 Benzenamine,/2-methyl-5-nitro­ 152 C7H8N2O2 000099-55-8 10 Abundance Scan 712 (11.578 min): 25040.D (-) m/z 149.90 100.00% i$o

5000

52 78 115 ..... j\... 11 20 11.40 11.60 11.80 12.00

m/z~> 30 40 50 60 ......... 1,1,,. m/z 151.90 68.61% 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

115 ,............ 5000 78 11 20 11.40 11.60 11.80 12.00 52 m/z 114.90 38.50% 35 I ■nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0

115 11.20 11,40 11,60 11.80 12.00 5000 52 78 m/z 78.05 19.48% fl 35 I I.... I,i,„ 4^ ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- .......... 77 106 1$2 11.20 11.40 11,60 11.80 12.00 m/z 52.00 ^13.98%

5000 51 94 66 ' I ‘ ' I ' ' ' ' I ' I'' I' I ■nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

25040.D NP103001.M Mon Nov 19 14:36:54 2001 Page 2

NYC-WTC_000069254

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NYC-WTC_000069254Source: NYC Law Department, mirrored locally

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